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Process Control

Efficient and cost-optimized operation of hard nip sizer using nonlinear modelling

June 1, 2021 By Henri Vaittinen, Antti Räisänen, Abhay Bulsari

##### By Henri Vaittinen and Antti Räisänen, Valmet Technologies, Järvenpää, Finland, and Abhay Bulsari, Nonlinear Solutions Oy, Turku, Finland

### Summary

Hard nip sizing increases strength properties of liner or fluting more than conventional sizing methods like film sizing or pond sizing.

When process variables of hard nip sizing are properly optimized, it becomes possible to improve quality and decrease raw material costs. For example, it becomes a lot easier to get more strength with less starch or fibres with hard nip sizing once quantitative information about the relations between strength and process variables is available.

These relations are not very simple or linear, which is why conventional linear statistical techniques are not very effective. However, as this article demonstrates amply, nonlinear modelling is a powerful tool for describing these relations. The nonlinear models are now used to calculate cost optimal operating conditions such that the final properties of liner board are within desired limits.

### Hard nip sizing process

Surface sizing is an essential process in the pulp and paper industry for improving the strength properties of base paper or board. In film sizing, the starch is applied mostly on the outer surfaces of the paper or board, and only a minor portion of the starch penetrates deep inside the structure of the base paper or board.

Hard nip sizing (Figure 1) overcomes this weakness by using considerably higher pressure, allowing for much deeper penetration of starch and other sizing chemicals [1], and thus increasing the strength properties more than conventional surface sizing processes. It also produces better smoothness because hard rolls work like in calendering.

As a matter of fact, hard nip sizer rolls and the loading system resemble more calenders than conventional sizer rolls. In hard nip sizing process, the high nip pressure results in an optimal packing of fibres and the sizing through the z-direction of the web, resulting in maximized increase of SCT in cross direction and burst strength [2].

A good process can be improved further by tuning it optimally. All processes can be made more efficient. That requires quantitative knowledge of the effects of several variables. Writing or creating such equations is called mathematical modelling.

### Mathematical modelling

Mathematical modelling can be performed in various ways, and different ways are suitable for different situations. Mathematical models represent knowledge of quantitative effects of relevant variables in a concise and precise form. They can be used instead of experimentation if they are reliable enough. Mathematical models also permit the user to carry out various kinds of calculations, like determining suitable values of variables, which will result in desired product quality in an economic way.

Physical or phenomenological modelling is not particularly effective for predicting material properties like strength, thermal conductivity or solubility. Physical modelling usually requires a lot of assumptions and simplifications. Empirical and semi-empirical modelling, on the other hand, does not need any major assumptions or simplifications. Empirical models simply describe the observed behaviour of a system. Empirical modelling is feasible when the relevant variables are measurable.

Conventional techniques of empirical modelling, however, are linear statistical techniques. These tend to have serious limitations because nothing in nature is very linear, and particularly so in process engineering and materials science. It therefore makes sense to use better techniques of empirical and semi-empirical modelling, which take nonlinearities into account.

### Nonlinear modelling

There is hardly any material behaviour that is absolutely linear. It is therefore wise to treat the nonlinearities rather than ignore them. Nonlinear modelling is empirical or semi-empirical modelling that takes at least some nonlinearities into account. Nonlinear modelling can be carried out with a variety of methods. The older techniques include polynomial regression, linear regression with nonlinear terms and nonlinear regression.

These techniques have several disadvantages compared to the new techniques of nonlinear modelling based on free-form nonlinearities, which do not require prior knowledge of the nonlinearities in the relations.

Among these new techniques, feed-forward neural networks have turned out to be particularly valuable in chemical engineering [3] and materials science. Besides their universal approximation capability [4], it is usually possible to produce nonlinear models with some extrapolation capabilities with feed-forward neural networks.

Neural networks have been in use in process industries for about 30 years [5]. The multilayer perceptron, a kind of a feed-forward neural network, is the most common one. Most neural network applications in industries are based on them [6-14]. Feed-forward neural networks consist of neurons in layers directionally connected to others in the adjacent layers (see Figure 2).

### Nonlinear modelling in process engineering

Nonlinear modelling has been utilized successfully for various industrial sectors including plastics [6], rubbers [7], metals [8], cement, concrete [9], medical materials [10], semiconductors [11], ceramics, glass [12], power [13], biotechnology [14], pulp, paper, etc.

Different processes have different characteristics – different raw materials, different compositions, and are produced by different batch, continuous or fed-batch processes. However, some things are common to modelling of various kinds of processes. Material properties or product properties, production rate and production economics depend on composition variables, process variables and dimension variables, as summarized in Figure 3.

Nonlinear models combined as shown in Figure 3 make process development a lot more efficient by drastically reducing expensive experimentation and by helping achieve better combinations of product properties, often optimized for cost.

### Experimentation

Nonlinear modelling needs either experimental or production data. With Valmet Technologies, an experimental approach was chosen with 83 carried out experiments. A much smaller number would have been sufficient for this work if the experiments had been planned keeping in mind that nonlinear models would be developed later. Besides SCT index and burst index, air porosity, thickness and density were also measured from each of the experiments.

The results from three experiments presented in Figure 4 show the effect of base paper’s basis weight on the increase in SCT index and burst index. The experimental data taken into use was consistent and of very good quality, and as a consequence, excellent nonlinear models could be developed.

The correlation coefficients of all the models were well above 90 per cent. It is natural that the nonlinear models perform very well since the effects are not very linear, while the linear models will not hesitate to predict even negative values of material properties.

### Nonlinear models of SCT index and burst index

After the data was analyzed to some extent, nonlinear models in the form of feed-forward neural networks were attempted using NLS 020 software to predict the increase in SCT index.

The input variables included basis weight of the base paper, size weight on top and bottom sides, the solids fractions in the sizing liquid, nip load, etc. It was possible to produce models with high correlation coefficients. The model selected for use had a correlation coefficient of 92.7 per cent and a standard deviation of prediction errors of 2.99 per cent (Figure 5). Similarly, nonlinear models were developed for burst index increase and for a few other properties including porosity.

The models were then implemented in LUMET system software, which allows various kinds of calculations from nonlinear models. Figure 6 shows the increase in SCT index against basis weight for different size weights. Figure 7 shows the increase in burst index against basis weight for different solids content on top side.

### Optimizing process conditions

Optimization helps derive the maximum benefit from the process. Once we have the quantitative knowledge of the process in the form of equations, it becomes possible to determine good operating conditions.

In this case, we would like to derive the maximum strength from a small amount of starch. Or we would like to minimize the operating cost and still derive a certain desired increase in strength. This has to be done in presence of constraints on several variables. The strength should not come at the cost of other properties. There are a lot of books that describe optimization methods [15] and are therefore not described here. However, this kind of calculations are now done with the nonlinear models implemented in a LUMET system, resulting in significant savings in starch.

### Conclusions

One can derive a lot more value from a process by tuning it well. Composition variables, process variables and dimension variables affect product properties in a complicated manner, and people with even decades of experience cannot predict the quantitative effects of the relevant variables. As clearly seen in this case, it is possible to get more strength with less applied starch in surface sizing.

A good process becomes better when tuned optimally, as in the case of hard nip sizing. Instead of trial and error experimentation, a small series of properly planned experiments makes it possible to derive the relevant quantitative information which is necessary to develop good nonlinear models.

### References

[1] J. Hakola, “Surface sizing with high nip pressure”, presented at the TAPPI conference 19PaperCon, Indianapolis, USA (May 2019)

[2] E. Pitschmann, “New technology HardNip PM1”, presented at the 28th International Munich Paper Symposium, Munich, Germany (March 2019)

[3] A. Bulsari (ed.), Neural Networks for Chemical Engineers, Elsevier, Amsterdam, 1995.

[4] K. Hornik, M. Stinchcombe, and H. White, “Multilayer feedforward networks are universal approximators”, Neural Networks, Vol. 2, (1989) 359-366.

[5] A. Bulsari, “Quality of nonlinear modelling in process industries”, Internal Report NLS/1998/2.

[6] A. Bulsari and M. Lahti, “How nonlinear models help improve the production economics of extrusion processes”, British Plastics and Rubber (September 2008) 30-32.

[7] A. Bulsari, J. Ilomäki, M. Lahtinen and R. Perkiö, “Nonlinear models of mechanical properties reduce rubber recipe development time”, Rubber World (September 2015) 28-33.

[8] A. Bulsari, H. Keife and J. Geluk, “Nonlinear models provide better control of annealed brass strip microstructure”, Advanced Materials and Processes (July 2012) 18-20.

[9] A. Bulsari, H. Kylmämetsä and K. Juvas, “Nonlinear models of workability and compressive strength help minimise costs”, Concrete Plant International, No. 6 (December 2009) 36-42.

[10] A. Bulsari, K. Lähteenkorva, E. Suokas and M. Huttunen, “Models add efficiency to bioabsorbable implant development”, Medical Design Technology, Vol. 19, No. 2 (March 2015) 26-28.

[11] A. Bulsari and V.-M. Airaksinen, “Nonlinear models used to address epi layer uniformity”, Solid State Technology, Vol. 47, No. 7 (July 2004) 33-38.

[12] A. Bulsari, P. Nurmi and M. Salonen, “Nonlinear models help to reduce production costs”, Glass Worldwide, No. 68 (November-December 2016) 118-119.

[13] A. Bulsari, A. Wemberg, A. Anttila and A. Multas, “Nonlinear models: coal combustion efficiency and emissions control”, Power Engineering International, Vol. 17, No. 4 (April 2009) 32-39.

[14] A. Bulsari, E. Kiljunen and M. Suhonen, “Speeding development of an enantioselective enzymatic process for a pharmaceutical intermediate”, BioProcess International, Vol. 5, No. 8 (September 2007) 52-63.

[15] P. E. Gill, W. Murray and M. H. Wright, Practical Optimisation, Academic Press, London (1981) 136-140.

*This paper was published in the Spring 2021 issue of *Pulp & Paper Canada*.*

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